Synthesis and characterization of lead zirconate titanate nanotubes

Jongok Kim; Yong Chan Choi; Sang Don Bu

doi:10.1080/00150190701512664

Synthesis and characterization of lead zirconate titanate nanotubes

Jongok Kim, Yong Chan Choi, Sang Don Bu

Division of Energy Techonology

Jeonbuk National University

Research output: Contribution to journal › Conference article › peer-review

5 Scopus citations

Abstract

We report a template-directed growth of Pb(Zrx,Ti_{1 x})O ₃ (PZT) nanotubes in conjunction with sol-gel process and spin coating technique. Field emission scanning electron microscope (FESEM) images show that PZT nanotubes are well packed inside the pore of a porous alumina membrane (PAM). A Field emission transmission electron microscope (FETEM) image of a freestanding PZT nanotube shows that its outer diameter and length are estimated to be 50 nm and several microns, respectively. High resolution FETEM analysis reveals that PZT nanotubes have a wall thickness of 5 nm and consist of crystallites with a size in the order of 2-3 nm. The occurrence of electron diffraction ring patterns confirms that the typical PZT nanotube is polycrystalline.

Original language	English
Pages (from-to)	236-241
Number of pages	6
Journal	Ferroelectrics
Volume	356
Issue number	1 PART 2
DOIs	https://doi.org/10.1080/00150190701512664
State	Published - 2007
Event	5th Asian Meeting on Ferroelectricity, AMF-5 - Noda, Japan Duration: 3 Sep 2006 → 7 Sep 2006

Bibliographical note

Funding Information:
This work was supported by the Korea Research Foundation through Grant funded by the Korean Government (MOEHRD) through Grant No. KRF-2006-312-C00136.

Keywords

Ferroelectric
Nanowire
Pb(Zr,Ti)O
Sol-gel
Spin coating

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10.1080/00150190701512664

Cite this

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title = "Synthesis and characterization of lead zirconate titanate nanotubes",

abstract = "We report a template-directed growth of Pb(Zrx,Ti1 x)O 3 (PZT) nanotubes in conjunction with sol-gel process and spin coating technique. Field emission scanning electron microscope (FESEM) images show that PZT nanotubes are well packed inside the pore of a porous alumina membrane (PAM). A Field emission transmission electron microscope (FETEM) image of a freestanding PZT nanotube shows that its outer diameter and length are estimated to be 50 nm and several microns, respectively. High resolution FETEM analysis reveals that PZT nanotubes have a wall thickness of 5 nm and consist of crystallites with a size in the order of 2-3 nm. The occurrence of electron diffraction ring patterns confirms that the typical PZT nanotube is polycrystalline.",

keywords = "Ferroelectric, Nanowire, Pb(Zr,Ti)O, Sol-gel, Spin coating",

author = "Jongok Kim and Choi, \{Yong Chan\} and Bu, \{Sang Don\}",

note = "Funding Information: This work was supported by the Korea Research Foundation through Grant funded by the Korean Government (MOEHRD) through Grant No. KRF-2006-312-C00136.; 5th Asian Meeting on Ferroelectricity, AMF-5 ; Conference date: 03-09-2006 Through 07-09-2006",

year = "2007",

doi = "10.1080/00150190701512664",

language = "English",

volume = "356",

pages = "236--241",

journal = "Ferroelectrics",

issn = "0015-0193",

publisher = "Taylor and Francis Ltd.",

number = "1 PART 2",

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TY - JOUR

T1 - Synthesis and characterization of lead zirconate titanate nanotubes

AU - Kim, Jongok

AU - Choi, Yong Chan

AU - Bu, Sang Don

N1 - Funding Information: This work was supported by the Korea Research Foundation through Grant funded by the Korean Government (MOEHRD) through Grant No. KRF-2006-312-C00136.

PY - 2007

Y1 - 2007

N2 - We report a template-directed growth of Pb(Zrx,Ti1 x)O 3 (PZT) nanotubes in conjunction with sol-gel process and spin coating technique. Field emission scanning electron microscope (FESEM) images show that PZT nanotubes are well packed inside the pore of a porous alumina membrane (PAM). A Field emission transmission electron microscope (FETEM) image of a freestanding PZT nanotube shows that its outer diameter and length are estimated to be 50 nm and several microns, respectively. High resolution FETEM analysis reveals that PZT nanotubes have a wall thickness of 5 nm and consist of crystallites with a size in the order of 2-3 nm. The occurrence of electron diffraction ring patterns confirms that the typical PZT nanotube is polycrystalline.

AB - We report a template-directed growth of Pb(Zrx,Ti1 x)O 3 (PZT) nanotubes in conjunction with sol-gel process and spin coating technique. Field emission scanning electron microscope (FESEM) images show that PZT nanotubes are well packed inside the pore of a porous alumina membrane (PAM). A Field emission transmission electron microscope (FETEM) image of a freestanding PZT nanotube shows that its outer diameter and length are estimated to be 50 nm and several microns, respectively. High resolution FETEM analysis reveals that PZT nanotubes have a wall thickness of 5 nm and consist of crystallites with a size in the order of 2-3 nm. The occurrence of electron diffraction ring patterns confirms that the typical PZT nanotube is polycrystalline.

KW - Ferroelectric

KW - Nanowire

KW - Pb(Zr,Ti)O

KW - Sol-gel

KW - Spin coating

UR - https://www.scopus.com/pages/publications/61449158343

U2 - 10.1080/00150190701512664

DO - 10.1080/00150190701512664

M3 - Conference article

AN - SCOPUS:61449158343

SN - 0015-0193

VL - 356

SP - 236

EP - 241

JO - Ferroelectrics

JF - Ferroelectrics

IS - 1 PART 2

T2 - 5th Asian Meeting on Ferroelectricity, AMF-5

Y2 - 3 September 2006 through 7 September 2006

ER -

Synthesis and characterization of lead zirconate titanate nanotubes

Abstract

Bibliographical note

Keywords

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