Structure evolution and properties in a rigid polyimide prepared from its flexible poly(amic acid) precursor

Moonhor Ree; Sung Ho Woo; Tae Joo Shin; Kyungjun Kim; Heesook Chang; Wang Cheol Zin; Ki Bong Lee; Yong Joon Park

doi:10.1002/masy.19971180130

Structure evolution and properties in a rigid polyimide prepared from its flexible poly(amic acid) precursor

Moonhor Ree, Sung Ho Woo, Tae Joo Shin, Kyungjun Kim, Heesook Chang, Wang Cheol Zin, Ki Bong Lee, Yong Joon Park

Division of Energy Techonology

Research output: Contribution to journal › Article › peer-review

13 Scopus citations

Abstract

Soluble poly(p-phenylene biphenyltetracarboxamic acid) precursor was converted to the polyimide by thermal imidization at various conditions. The structure evolution being occurred during its thermal imidization over 25-400°C was investigated as a function of imidization temperature and time by X-ray scattering with synchrotron radiation sources of Pohang Accelerator Laboratory in Korea and with conventional radiation sources. In addition, properties in the polyimide films were investigated by dynamic mechanical thermal analysis, stress-strain analysis, prism coupling, and residual stress analysis.

Original language	English
Pages (from-to)	213-220
Number of pages	8
Journal	Macromolecular Symposia
Volume	118
DOIs	https://doi.org/10.1002/masy.19971180130
State	Published - Jun 1997

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title = "Structure evolution and properties in a rigid polyimide prepared from its flexible poly(amic acid) precursor",

abstract = "Soluble poly(p-phenylene biphenyltetracarboxamic acid) precursor was converted to the polyimide by thermal imidization at various conditions. The structure evolution being occurred during its thermal imidization over 25-400°C was investigated as a function of imidization temperature and time by X-ray scattering with synchrotron radiation sources of Pohang Accelerator Laboratory in Korea and with conventional radiation sources. In addition, properties in the polyimide films were investigated by dynamic mechanical thermal analysis, stress-strain analysis, prism coupling, and residual stress analysis.",

author = "Moonhor Ree and Woo, \{Sung Ho\} and Shin, \{Tae Joo\} and Kyungjun Kim and Heesook Chang and Zin, \{Wang Cheol\} and Lee, \{Ki Bong\} and Park, \{Yong Joon\}",

year = "1997",

month = jun,

doi = "10.1002/masy.19971180130",

language = "English",

volume = "118",

pages = "213--220",

journal = "Macromolecular Symposia",

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T1 - Structure evolution and properties in a rigid polyimide prepared from its flexible poly(amic acid) precursor

AU - Ree, Moonhor

AU - Woo, Sung Ho

AU - Shin, Tae Joo

AU - Kim, Kyungjun

AU - Chang, Heesook

AU - Zin, Wang Cheol

AU - Lee, Ki Bong

AU - Park, Yong Joon

PY - 1997/6

Y1 - 1997/6

N2 - Soluble poly(p-phenylene biphenyltetracarboxamic acid) precursor was converted to the polyimide by thermal imidization at various conditions. The structure evolution being occurred during its thermal imidization over 25-400°C was investigated as a function of imidization temperature and time by X-ray scattering with synchrotron radiation sources of Pohang Accelerator Laboratory in Korea and with conventional radiation sources. In addition, properties in the polyimide films were investigated by dynamic mechanical thermal analysis, stress-strain analysis, prism coupling, and residual stress analysis.

AB - Soluble poly(p-phenylene biphenyltetracarboxamic acid) precursor was converted to the polyimide by thermal imidization at various conditions. The structure evolution being occurred during its thermal imidization over 25-400°C was investigated as a function of imidization temperature and time by X-ray scattering with synchrotron radiation sources of Pohang Accelerator Laboratory in Korea and with conventional radiation sources. In addition, properties in the polyimide films were investigated by dynamic mechanical thermal analysis, stress-strain analysis, prism coupling, and residual stress analysis.

UR - https://www.scopus.com/pages/publications/0031478040

U2 - 10.1002/masy.19971180130

DO - 10.1002/masy.19971180130

M3 - Article

AN - SCOPUS:0031478040

SN - 1022-1360

VL - 118

SP - 213

EP - 220

JO - Macromolecular Symposia

JF - Macromolecular Symposia

ER -

Structure evolution and properties in a rigid polyimide prepared from its flexible poly(amic acid) precursor

Abstract

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